1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate

Base Information

• Chemical Name: 1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate
• CAS No.: 943321-55-9
• Molecular Formula: C₂₅H₂₆N₄O₃S
• Molecular Weight: 462.572

Synonyms:1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate

Chemical Property of 1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate

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Technology Process of 1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate

There total 1 articles about 1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

1,1-dimethylethyl {2-phenyl-2-[({5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}carbonyl)amino]ethyl}carbamate (943321-54-8) → 1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate (943321-55-9)

Guidance literature:

With methanol; sodium hydroxide; In tetrahydrofuran; water; at 25 - 50 ℃; for 2h;

Reference yield: 100.0%

1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate (943321-55-9) → C20H18N4OS (943321-51-5)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃;

DOI:10.1016/j.bmcl.2009.02.094

Reference yield: 34.0%

1,1-dimethylethyl [2-phenyl-2-({[5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thienyl]carbonyl}amino)ethyl]carbamate (943321-55-9) → N-(2-amino-1-phenylethyl)-5-(1H-pyrrolo[2,3-b]pyridin-4-yl)-2-thiophenecarboxamide dihydrochloride

Guidance literature:

With hydrogenchloride; methanol; In 1,4-dioxane; for 12h;

upstream raw materials:

1,1-dimethylethyl {2-phenyl-2-[({5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}carbonyl)amino]ethyl}carbamate

Downstream raw materials:

C₂₀H₁₈N₄OS

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