ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside
CAS No.:189188-22-5
Molecular Formula:C₂₅H₂₇NO₈S₂
Molecular Weight:533.623
Hs Code.:

Synonyms:ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

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Chemical Property of ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

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Technology Process of ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

There total 4 articles about ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 189188-21-4
ethyl 3-O-acetyl-2,6-dideoxy-6-iodo-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

: 189188-22-5
ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; for 2h;
DOI:10.1016/S0040-4020(97)00145-2

Reference yield:

: 189188-19-0
ethyl 3-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 189188-22-5
ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / pyridine / 96 h / Ambient temperature

2: 69 percent / NaI / butan-2-one / 16 h / Heating

3: 86 percent / H₂, Et₃N / Pd/C / ethanol / 2 h

With pyridine; hydrogen; triethylamine; sodium iodide; palladium on activated charcoal; In ethanol; butanone;
DOI:10.1016/S0040-4020(97)00145-2

Reference yield:

: ethyl 3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-1-thio-β-D-glucopyranoside

: 189188-22-5
ethyl 3-O-acetyl-2,6-dideoxy-2-phthalimido-1-thio-4-O-(4-toluenesulfonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / CF₃CO₂H, H₂O / CH₂Cl₂ / 2 h / 20 °C

2: 77 percent / pyridine / 96 h / Ambient temperature

3: 69 percent / NaI / butan-2-one / 16 h / Heating

4: 86 percent / H₂, Et₃N / Pd/C / ethanol / 2 h

With pyridine; water; hydrogen; triethylamine; trifluoroacetic acid; sodium iodide; palladium on activated charcoal; In ethanol; dichloromethane; butanone;
DOI:10.1016/S0040-4020(97)00145-2