3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

Base Information

Chemical Name:3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate
CAS No.:392620-76-7
Molecular Formula:C₃₀H₃₇NO₇SSi
Molecular Weight:583.778
Hs Code.:

Synonyms:3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

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Chemical Property of 3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

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Technology Process of 3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

There total 5 articles about 3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 392620-72-3
4-{[tert-Butyl(diphenyl)silyl]oxy}-3-[(methylsulfonyl)amino]phenyl acetate

: 392620-76-7
3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

Guidance literature:: In dichloromethane;
DOI:10.1016/S0960-894X(01)00645-X

Reference yield:

: 392620-63-2
acetic acid 3-nitro-4-(tert-butyl-diphenyl-silanyloxy)-phenyl ester

: 392620-76-7
3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / H₂ / Raney Ni / tetrahydrofuran

2: 66 percent / iPr₂NEt / tetrahydrofuran

3: 96 percent / CH₂Cl₂

With hydrogen; N-ethyl-N,N-diisopropylamine; nickel; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0960-894X(01)00645-X

Reference yield:

: 6322-56-1
4'-hydroxy-3'-nitroacetophenone

: 392620-76-7
3-[(tert-Butoxycarbonyl)(methylsulfonyl)amino]-4-{[tert-butyl(diphenyl)-silyl]oxy}phenyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / imidazole / CH₂Cl₂

2: 85 percent / MCPBA / CHCl₃

3: 73 percent / H₂ / Raney Ni / tetrahydrofuran

4: 66 percent / iPr₂NEt / tetrahydrofuran

5: 96 percent / CH₂Cl₂

With 1H-imidazole; hydrogen; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; nickel; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1016/S0960-894X(01)00645-X