1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

Base Information

Chemical Name:1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane
CAS No.:1268342-45-5
Molecular Formula:C₂₂H₁₈F₆N₆S₂
Molecular Weight:544.548
Hs Code.:

Synonyms:1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

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Chemical Property of 1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

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Technology Process of 1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

There total 4 articles about 1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1158982-19-4
2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)benzenesulfonyl chloride

: 1268342-45-5
1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

Guidance literature:: With hydrogenchloride; iron; In water; acetic acid; at 120 ℃;

Reference yield: 71.94%

: 1158982-22-9
2,4-dimethyl-5-(3-trifluoromethyl-1H-1,2,4-triazol-1-yl)thiophenol

: 1268342-45-5
1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

Guidance literature:: With iron; for 3h;

Reference yield:

: 55499-44-0
2,4-dimethylbenzeneboronic acid

: 1268342-45-5
1,2-bis(2,4-dimethyl-5-(3-(trifluoromethyl)-1H-1,2,4-triazol-1-yl)phenyl)disulfane

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / copper / N,N-dimethyl-formamide / 4 h / 50 °C

2: chlorosulfonic acid / 3 h / 70 °C / Inert atmosphere

3: hydrogenchloride / iron / water; acetic acid / 120 °C

With pyridine; hydrogenchloride; chlorosulfonic acid; iron; copper; In water; acetic acid; N,N-dimethyl-formamide;