Technology Process of benzyl 3-phenylbenzofuran-2-ylcarbamate
There total 5 articles about benzyl 3-phenylbenzofuran-2-ylcarbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; cesium fluoride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
1,1-dimethoxyethane; water;
for 10h;
Inert atmosphere;
Reflux;
DOI:10.1021/jo102265b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide; sodium t-butanolate / 1,2-dimethoxyethane / 20 h / 75 °C / Inert atmosphere
2: N-Bromosuccinimide; toluene-4-sulfonic acid / tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere; Darkness
3: palladium diacetate; cesium fluoride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,1-dimethoxyethane; water / 10 h / Inert atmosphere; Reflux
With
N-Bromosuccinimide; sodium azide; palladium diacetate; toluene-4-sulfonic acid; cesium fluoride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate;
In
tetrahydrofuran; 1,2-dimethoxyethane; 1,1-dimethoxyethane; water;
1: Curtius rearrangement / 3: Suzuki-Miyaura reaction;
DOI:10.1021/jo102265b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / tetrahydrofuran / 16 h / Inert atmosphere; Reflux
2: N-Bromosuccinimide; toluene-4-sulfonic acid / tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere; Darkness
3: palladium diacetate; cesium fluoride; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,1-dimethoxyethane; water / 10 h / Inert atmosphere; Reflux
With
dmap; N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid; cesium fluoride; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene;
In
tetrahydrofuran; 1,1-dimethoxyethane; water;
3: Suzuki-Miyaura reaction;
DOI:10.1021/jo102265b
