bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane

Base Information Edit

Chemical Name:bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane
CAS No.:186381-20-4
Molecular Formula:C₃₁H₃₀N₆O₆
Molecular Weight:582.616
Hs Code.:
Mol file:186381-20-4.mol

Synonyms:bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane

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Chemical Property of bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane Edit

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Technology Process of bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane

There total 2 articles about bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4434-13-3
2-carboxy-5-methylpyridine

: 186381-20-4
bis[3-nitro-4-[ethyl[(5-methylpyridin-2-yl)carbonyl]amino]phenyl]methane

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CH₂Cl₂; dimethylformamide / 1 h / Heating

2: 650 mg / Et₃N / CH₂Cl₂ / 18 h / Heating

With thionyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Chlorination / 2: Acylation;
DOI:10.1021/ja963693l