Technology Process of 3-((3E,7E,11E)-4-ethyl-8,12,16-trimethyl-6-(phenylsulfonyl)heptadeca-3,7,11,15-tetraen-1-yl)furan
There total 7 articles about 3-((3E,7E,11E)-4-ethyl-8,12,16-trimethyl-6-(phenylsulfonyl)heptadeca-3,7,11,15-tetraen-1-yl)furan which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(E)-3-[4-bromomethylhex-3-enyl]furan; (E,E)-farnesyl phenylsulfone;
With
potassium tert-butylate;
In
tetrahydrofuran;
at -30 ℃;
for 1h;
Inert atmosphere;
With
ammonium chloride;
In
tetrahydrofuran; water;
Inert atmosphere;
DOI:10.1016/j.tet.2011.05.009
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / 0 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
3.1: potassium tert-butylate / tetrahydrofuran / 1 h / -30 °C / Inert atmosphere
3.2: Inert atmosphere
With
carbon tetrabromide; potassium tert-butylate; diisobutylaluminium hydride; triphenylphosphine;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/j.tet.2011.05.009
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.1: potassium tert-butylate / tetrahydrofuran / 1 h / -30 °C / Inert atmosphere
2.2: Inert atmosphere
With
carbon tetrabromide; potassium tert-butylate; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2011.05.009
![(E)-3-[4-bromomethylhex-3-enyl]furan](/Databaselist/images/loading.webp)
