1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

Base Information

Chemical Name:1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane
CAS No.:372112-71-5
Molecular Formula:C₃₆H₃₂FPSi₂
Molecular Weight:570.793
Hs Code.:

Synonyms:1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

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Chemical Property of 1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

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Technology Process of 1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

There total 4 articles about 1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1,1-difluoro-1,2-dimethyl-2,2-diphenyldisilane

: 321148-68-9
(8-bromo-naphth-1-yl)di(phenyl)phosphine

: 372112-71-5
1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

Guidance literature:: (8-bromo-naphth-1-yl)di(phenyl)phosphine; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 1h;

1,1-difluoro-1,2-dimethyl-2,2-diphenyldisilane; In diethyl ether; hexane; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/ja0160602

Reference yield:

: 4044-58-0
1-bromo-8-iodo-naphthalene

: 372112-71-5
1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / 0.03 h / -78 °C

1.2: 4 h / -78 °C

2.1: n-BuLi / diethyl ether; hexane / 1 h / 0 °C

2.2: 84 percent / diethyl ether; hexane / 12 h / 20 °C

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ja0160602

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 372112-71-5
1-fluoro-1,2-dimethyl-2,2-diphenyl-1-[8-(diphenylphosphino)-1-naphthyl]disilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / 0.03 h / -78 °C

1.2: 4 h / -78 °C

2.1: n-BuLi / diethyl ether; hexane / 1 h / 0 °C

2.2: 84 percent / diethyl ether; hexane / 12 h / 20 °C

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ja0160602