3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

Base Information

Chemical Name:3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene
CAS No.:120125-75-9
Molecular Formula:C₁₆H₁₂Cl₃FO₄
Molecular Weight:393.626
Hs Code.:

Synonyms:3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

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Chemical Property of 3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

Chemical Property:

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Technology Process of 3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

There total 5 articles about 3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.8%

: 103843-71-6
1-benzyloxy-3,4-dichloro-2-(2,3-epoxypropoxy)-5-(2-fluorobenzoyl)benzene

: 120125-75-9
3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

Guidance literature:: With hydrogenchloride; for 6h; Heating;
DOI:10.1248/cpb.36.3404

Reference yield:

: 3978-67-4
3,4-dichloro-1,2-benzenediol

: 120125-75-9
3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) AlCl₃, 2.) 2 N NaOH / 1.) 1,2-dichloroethane, reflux, 24 h, 2.) EtOH, reflux, 30 min

2: 71.4 percent / NaH / dimethylformamide / 0.25 h / Ambient temperature

3: 91.9 percent / NaH / dimethylformamide / 23 h / 80 °C

4: 67.8 percent / conc. HCl / 6 h / Heating

With hydrogenchloride; sodium hydroxide; aluminium trichloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3404

Reference yield:

: 103843-57-8
3,4-dichloro-5-(2-fluorobenzoyl)-1,2-dihydroxybenzene

: 120125-75-9
3,4-dichloro-2-(3-chloro-2-hydroxypropoxy)-5-(2-fluorobenzoyl)-1-hydroxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 71.4 percent / NaH / dimethylformamide / 0.25 h / Ambient temperature

2: 91.9 percent / NaH / dimethylformamide / 23 h / 80 °C

3: 67.8 percent / conc. HCl / 6 h / Heating

With hydrogenchloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3404