Technology Process of 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]cholestan
There total 1 articles about 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]cholestan which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Cholestanol; 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate;
In
dichloromethane;
for 1h;
Molecular sieve;
Inert atmosphere;
With
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 ℃;
for 3h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.10.015
