3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

Base Information

Chemical Name:3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene
CAS No.:1313574-14-9
Molecular Formula:C₃₉H₂₈OP₂
Molecular Weight:574.598
Hs Code.:

Synonyms:3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

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Chemical Property of 3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

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Technology Process of 3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

There total 1 articles about 3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 13461-74-0
9-ethynylfluoren-9-ol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1313574-14-9
3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

Guidance literature:: With triethylamine; In dichloromethane; pentane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/om200357v

Reference yield: 96.0%

: 1313574-14-9
3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

: 1313574-15-0
3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphinyl)-1-(diphenylthiophosphinyl)allene

Guidance literature:: With sulfur; In toluene; at 20 ℃; for 46h; Inert atmosphere;
DOI:10.1021/om200357v

Reference yield: 76.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 1313574-14-9
3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene

: [κ2-P,O-3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene]dichloropalladium*(chloroform)

: bis[κ1-P-3,3-(biphenyl-2,2'-diyl)-1-(diphenylphosphino)-1-(diphenylphosphinyl)allene]tetrachlorodipalladium*(chloroform)

Guidance literature:: In dichloromethane; under N2; solid Pd complex added to soln. of ligand in dry CH2Cl2; stirred at room temp. for 1 h; volatiles removed; washed with small amt. of ether and then pentane; elem. anal.;
DOI:10.1021/om200357v