trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

Base Information

Chemical Name:trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester
CAS No.:245556-84-7
Molecular Formula:C₃₅H₃₆O₄
Molecular Weight:520.668
Hs Code.:

Synonyms:trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

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Chemical Property of trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

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Technology Process of trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

There total 1 articles about trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 2969-81-5
Ethyl 4-bromobutyrate

: 185223-78-3
(E,Z)-1-[4-(benzyloxy)phenyl]-1-(4-hydroxyphenyl)-2-phenylbut-1-ene

: 245556-84-7
trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

Guidance literature:: In acetone; for 10h; Heating;
DOI:10.1021/jm990078u

Reference yield: 65.0%

: 245556-84-7
trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

: 4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 1h; Ambient temperature;
DOI:10.1021/jm990078u

Reference yield:

: 245556-84-7
trans-4-<<1-(4-benzyloxyphenyl)-2-phenyl-1-butenyl>phenoxy>-n-butanoic acid ethyl ester

: 4-<<1-(4-hydroxyphenyl)-2-phenyl-1-butanyl>phenoxy>-n-butanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. NaOH / dioxane / 1 h / Ambient temperature

2: 42 percent / H₂ / 10 percent Pd/C / tetrahydrofuran / 24 h / 2275.45 Torr

With sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jm990078u