C₃₁H₃₄F₂N₈O₂

Base Information

Chemical Name:C₃₁H₃₄F₂N₈O₂
CAS No.:618892-77-6
Molecular Formula:C₃₁H₃₄F₂N₈O₂
Molecular Weight:588.66
Hs Code.:

C<sub>31</sub>H<sub>34</sub>F<sub>2</sub>N<sub>8</sub>O<sub>2</sub>

Synonyms:C₃₁H₃₄F₂N₈O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₄F₂N₈O₂

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Technology Process of C₃₁H₃₄F₂N₈O₂

There total 9 articles about C₃₁H₃₄F₂N₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₃₆H₄₂F₂N₈O₄

: 618892-77-6
C₃₁H₃₄F₂N₈O₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

Reference yield:

: 695-34-1
2-Amino-4-methylpyridine

: 618892-77-6
C₃₁H₃₄F₂N₈O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tert-butyl alcohol / 15 h / 23 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 23 °C

2.2: 48 h / -78 - 23 °C

3.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C

4.1: acetic acid / dichloromethane / 0.67 h / 23 °C

4.2: 15 h / 23 °C

5.1: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 23 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 24 h / 20 - 50 °C

7.1: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

With lithium hydroxide; sodium hypochlorite; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 618900-75-7
C₂₂H₂₃F₂N₅O₃

: 618892-77-6
C₃₁H₃₄F₂N₈O₂

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl iodide / chloroform / 0.33 h / 20 - 50 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 24 h / 20 - 50 °C

3: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

With trimethylsilyl iodide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; N,N-dimethyl-formamide;