Technology Process of C32H35N7O8
There total 9 articles about C32H35N7O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
DMF (N,N-dimethyl-formamide);
at 20 ℃;
for 10h;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: acetic acid / 5 h / Heating / reflux
2: triethylamine / methanol / 4 h / Heating / reflux
3: trichlorophosphate / 1.5 h / 10 - 60 °C
4: triethylamine / isopropyl alcohol / 2 h / Heating / reflux
5: ethylene glycol / 2 h / Heating / reflux
6: tetra-(n-butyl)ammonium iodide; potassium carbonate / DMF (N,N-dimethyl-formamide) / 48 h / 20 °C
7: di-isopropyl azodicarboxylate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 0 - 20 °C
8: methanol; hydrazine / 0.05 h / Heating / reflux
9: DMF (N,N-dimethyl-formamide) / 10 h / 20 °C
With
methanol; di-isopropyl azodicarboxylate; tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; triphenylphosphine; hydrazine; trichlorophosphate;
In
methanol; DMF (N,N-dimethyl-formamide); ethylene glycol; acetic acid; isopropyl alcohol;
4: Knoevenagel Condensation / 7: Mitsunobu reaction;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: triethylamine / methanol / 4 h / Heating / reflux
2: trichlorophosphate / 1.5 h / 10 - 60 °C
3: triethylamine / isopropyl alcohol / 2 h / Heating / reflux
4: ethylene glycol / 2 h / Heating / reflux
5: tetra-(n-butyl)ammonium iodide; potassium carbonate / DMF (N,N-dimethyl-formamide) / 48 h / 20 °C
6: di-isopropyl azodicarboxylate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 0 - 20 °C
7: methanol; hydrazine / 0.05 h / Heating / reflux
8: DMF (N,N-dimethyl-formamide) / 10 h / 20 °C
With
methanol; di-isopropyl azodicarboxylate; tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; triphenylphosphine; hydrazine; trichlorophosphate;
In
methanol; DMF (N,N-dimethyl-formamide); ethylene glycol; isopropyl alcohol;
3: Knoevenagel Condensation / 6: Mitsunobu reaction;