2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

Base Information

Chemical Name:2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine
CAS No.:303743-62-6
Molecular Formula:C₁₅H₂₅N₃O₂
Molecular Weight:279.382
Hs Code.:

Synonyms:2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

Chemical Property:

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Technology Process of 2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

There total 3 articles about 2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 619-22-7
3-(dimethylamino)benzaldehyde

: 303743-62-6
2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

Guidance literature:: With 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate; In ethanol; Heating;
DOI:10.1021/ja994547t

Reference yield:

: 23501-93-1
3-dimethylaminobenzyl alcohol

: 303743-62-6
2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / pyridinium chlorochromate; pyridine; Na₂CO₃ / CH₂Cl₂ / Heating

2: 85 percent / 2,3-bis(hydroxylamino)-2,3-dimethylbutane sulfate / ethanol / Heating

With pyridine; sodium carbonate; 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate; pyridinium chlorochromate; In ethanol; dichloromethane;
DOI:10.1021/ja994547t

Reference yield:

: 16518-64-2
3-(dimethylamino)benzoic acid methyl ester

: 303743-62-6
2-(3'-dimethylaminophenyl)-1,3-dihydroxy-4,4,5,5-tetramethylimidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / LiAlH₄ / diethyl ether / 3 h / Heating

2: 5 percent / pyridinium chlorochromate; pyridine; Na₂CO₃ / CH₂Cl₂ / Heating

3: 85 percent / 2,3-bis(hydroxylamino)-2,3-dimethylbutane sulfate / ethanol / Heating

With pyridine; lithium aluminium tetrahydride; sodium carbonate; 2,3-bis(hydroxyamino)-2,3-dimethylbutane monosulfate; pyridinium chlorochromate; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ja994547t