C₁₈H₂₄O₄

Base Information

Chemical Name:C₁₈H₂₄O₄
CAS No.:1449483-43-5
Molecular Formula:C₁₈H₂₄O₄
Molecular Weight:304.386
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>4</sub>

Synonyms:C₁₈H₂₄O₄

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Chemical Property of C₁₈H₂₄O₄

Chemical Property:

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Technology Process of C₁₈H₂₄O₄

There total 16 articles about C₁₈H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1392307-76-4
(1S,2R,3R,4R,5R)-methyl 3-(benzyloxy)-4-(tert-butyldimethylsilyloxy)-5-methyl-2-vinylcyclohexanecarboxylate

: 1449483-43-5
C₁₈H₂₄O₄

Guidance literature:: With hydrogen fluoride; In acetonitrile; at 40 ℃; for 96h;
DOI:10.1039/c3ob40692j

Reference yield:

: (S)-4-benzyl-3-((2S,3R,4R)-2-(benzyloxy)-3-(tert-butyldimethylsilyloxy)-4,8-dimethylnon-7-enoyl)oxazolidin-2-one

: 1449483-43-5
C₁₈H₂₄O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium tetrahydroborate / water; tetrahydrofuran / 20 h / 0 - 20 °C

2.1: Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C

2.2: 20 h / 20 °C

3.1: diisobutylaluminium hydride / toluene; diethyl ether / 0.25 h / -40 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -10 °C

6.1: periodic acid dihydrate / diethyl ether / 0.25 h

7.1: triphenylphosphine; pyrrolidine; palladium diacetate / dimethyl sulfoxide / 20 °C

8.1: Oxone / N,N-dimethyl-formamide / 18 h / 20 °C

9.1: diethyl ether / 0.25 h / 0 °C

10.1: hydrogen fluoride / acetonitrile / 96 h / 40 °C

With pyrrolidine; dmap; Oxone; sodium tetrahydroborate; periodic acid dihydrate; hydrogen fluoride; palladium diacetate; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1039/c3ob40692j

Reference yield:

: 1392307-50-4
(2R,3R,4R)-2-(benzyloxy)-3-(tert-butyldimethylsilyloxy)-4,8-dimethylnon-7-en-1-ol

: 1449483-43-5
C₁₈H₂₄O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C

1.2: 20 h / 20 °C

2.1: diisobutylaluminium hydride / toluene; diethyl ether / 0.25 h / -40 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 20 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -10 °C

5.1: periodic acid dihydrate / diethyl ether / 0.25 h

6.1: triphenylphosphine; pyrrolidine; palladium diacetate / dimethyl sulfoxide / 20 °C

7.1: Oxone / N,N-dimethyl-formamide / 18 h / 20 °C

8.1: diethyl ether / 0.25 h / 0 °C

9.1: hydrogen fluoride / acetonitrile / 96 h / 40 °C

With pyrrolidine; dmap; Oxone; periodic acid dihydrate; hydrogen fluoride; palladium diacetate; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1039/c3ob40692j