(o-methoxyphenyl)thionoarsine

Base Information

• Chemical Name: (o-methoxyphenyl)thionoarsine
• CAS No.: 131367-85-6
• Molecular Formula: C₇H₇AsOS
• Molecular Weight: 214.12

Synonyms:(o-methoxyphenyl)thionoarsine

Chemical Property of (o-methoxyphenyl)thionoarsine

Chemical Property:

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Technology Process of (o-methoxyphenyl)thionoarsine

There total 5 articles about (o-methoxyphenyl)thionoarsine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2,4-Bis-(2-methoxy-phenyl)-1,3-diphenyl-[1,3,2,4]diazadiarsetidine (125931-64-8) → (o-methoxyphenyl)thionoarsine (131367-85-6) + Azobenzene (1227476-15-4)

Guidance literature:

With sulfur; at 160 ℃; for 2h; other diazadiarsetidines;

Reference yield: 77.0%

1,3-di-tert-butyl-2,4-bis(o-methoxyphenyl)-1,3,2,4-diazadiarsetidine (125910-97-6) → N,N-di-tert-butylthiourea (4041-95-6) + (o-methoxyphenyl)thionoarsine (131367-85-6)

Guidance literature:

With carbon disulfide; at 40 ℃; for 4h; other diazadiarsetidines;

Reference yield:

1,3-di-tert-butyl-2,4-bis(o-methoxyphenyl)-1,3,2,4-diazadiarsetidine (125910-97-6) → (o-methoxyphenyl)thionoarsine (131367-85-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 42 percent / Heating

2: sulfur

With sulfur;

upstream raw materials:

1,3-di-tert-butyl-2,4-bis(o-methoxyphenyl)-1,3,2,4-diazadiarsetidine

2,4-Bis-(2-methoxy-phenyl)-1,3-diphenyl-[1,3,2,4]diazadiarsetidine

1,3-bis(p-bromophenyl)-2,4-bis(o-methoxyphenyl)-1,3,2,4-diazadiarsetidine

tetrakis(o-methoxyphenyl)-1,3,2,4-diazadiarsetidine

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