5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

Base Information

• Chemical Name: 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene
• CAS No.: 177079-03-7
• Molecular Formula: C₁₀H₁₅NO₄
• Molecular Weight: 213.233
• Mol file: 177079-03-7.mol

Synonyms:5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

Chemical Property of 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

There total 1 articles about 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene (177079-03-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 46 percent / CsF / acetonitrile; dimethylformamide / Heating

2: 72 percent / H₂ / Pd(OH)2/C / acetic acid / 50 °C / 7600 Torr

3: 80 percent / KOH / ethane-1,2-diol / 190 °C

With potassium hydroxide; hydrogen; cesium fluoride; palladium dihydroxide; In ethylene glycol; acetic acid; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1016/0040-4039(96)00509-6

upstream raw materials:

triethylene glycol di-(p-toluenesulfonate)