5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

Base Information

Chemical Name:5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene
CAS No.:177079-03-7
Molecular Formula:C₁₀H₁₅NO₄
Molecular Weight:213.233
Hs Code.:

Synonyms:5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

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Chemical Property of 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

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Technology Process of 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

There total 1 articles about 5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 177079-03-7
5,6,8,9,11,12-Hexahydro-2H-4,7,10,13-tetraoxa-2-aza-cyclopentacyclododecene

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / CsF / acetonitrile; dimethylformamide / Heating

2: 72 percent / H₂ / Pd(OH)2/C / acetic acid / 50 °C / 7600 Torr

3: 80 percent / KOH / ethane-1,2-diol / 190 °C

With potassium hydroxide; hydrogen; cesium fluoride; palladium dihydroxide; In ethylene glycol; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(96)00509-6