2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide

Base Information

• Chemical Name: 2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide
• CAS No.: 1067652-25-8
• Molecular Formula: C₂₇H₃₃F₂N₅O₅
• Molecular Weight: 545.586

Synonyms:2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide

Chemical Property of 2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide

Chemical Property:

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Technology Process of 2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide

There total 2 articles about 2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-O-allyl-5-azido-3,5-dideoxy-6-O-(3,5-difluorophenyl)-L-lyxo-1,4-lactone (1067652-24-7) + L-valine benzylamide (106566-02-3,120369-25-7,144902-31-8) → 2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide (1067652-25-8)

Guidance literature:

With 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine; at 70 ℃;

DOI:10.1016/j.bmc.2009.12.051

Reference yield: 77.0%

→ 2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide (1067652-25-8)

Guidance literature:

Reference yield:

2-allyloxy-5-azido-6-(3,5-difluoro-phenoxy)-4-hydroxyhexanoic acid (1-benzylcarbamoyl-2-methyl-propyl)-amide (1067652-25-8) → C27H37F2N3O5 (1067652-66-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 760.051 Torr;

upstream raw materials:

2-O-allyl-5-azido-3,5-dideoxy-6-O-(3,5-difluorophenyl)-L-lyxo-1,4-lactone

L-valine benzylamide

Downstream raw materials:

C₂₇H₃₅F₂N₃O₅

C₂₇H₃₇F₂N₃O₅

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