methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside
CAS No.:1402224-15-0
Molecular Formula:C₅₃H₅₆ClN₃O₂₀
Molecular Weight:1090.49
Hs Code.:

methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

Synonyms:methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

There total 3 articles about methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402224-14-9
methyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-D-glucopyranosyl-(1→3)-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

: 1402224-15-0
methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

: 1402224-16-1
C₅₃H₅₆ClN₃O₂₀

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; at 4 - 20 ℃; for 1.5h; Molecular sieve;
DOI:10.1016/j.carres.2012.07.019

Reference yield:

: 2,4-di-O-acetyl-6-О-chloroacetyl-3-О-(2,3,4-tri-О-benzoyl-α-L-rhamnopyranosyl)-α-D-glucopyranosyl trichloroacetimidate

: 1402224-15-0
methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

: 1402224-16-1
C₅₃H₅₆ClN₃O₂₀

Guidance literature:: Multi-step reaction with 2 steps

1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / -40 - -30 °C / Molecular sieve; Inert atmosphere

2: hydrogenchloride; sodium cyanoborohydride / 1,4-dioxane; tetrahydrofuran / 1.5 h / 4 - 20 °C / Molecular sieve

With hydrogenchloride; di-n-butylboryl trifluoromethanesulfonate; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.carres.2012.07.019

Reference yield:

: 2,4-di-O-acetyl-6-О-chloroacetyl-3-О-(2,3,4-tri-О-benzoyl-β-L-rhamnopyranosyl)-D-glucopyranose

: 1402224-15-0
methyl 2,3,4-tri-O-benzoyl-α-l-rhamnopyranosyl-(1→3)-2,4-di-O-acetyl-6-О-chloroacetyl-β-d-glucopyranosyl-(1→3)-2-azido-6-O-benzyl-2-deoxy-α-d-galactopyranoside

: 1402224-16-1
C₅₃H₅₆ClN₃O₂₀

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1.5 h / -18 - 20 °C

2: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / -40 - -30 °C / Molecular sieve; Inert atmosphere

3: hydrogenchloride; sodium cyanoborohydride / 1,4-dioxane; tetrahydrofuran / 1.5 h / 4 - 20 °C / Molecular sieve

With hydrogenchloride; di-n-butylboryl trifluoromethanesulfonate; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.carres.2012.07.019