2-nitro-4-decyldiazobenzene tetrafluoroborate

Base Information

Chemical Name:2-nitro-4-decyldiazobenzene tetrafluoroborate
CAS No.:1598408-16-2
Molecular Formula:BF₄*C₁₆H₂₄N₃O₂
Molecular Weight:377.19
Hs Code.:

Synonyms:2-nitro-4-decyldiazobenzene tetrafluoroborate

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Chemical Property of 2-nitro-4-decyldiazobenzene tetrafluoroborate

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Technology Process of 2-nitro-4-decyldiazobenzene tetrafluoroborate

There total 3 articles about 2-nitro-4-decyldiazobenzene tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: tetrafluoroboric acid

: 118788-66-2
n-decyl-4 nitro-2 aniline

: 1598408-16-2
2-nitro-4-decyldiazobenzene tetrafluoroborate

Guidance literature:: tetrafluoroboric acid; n-decyl-4 nitro-2 aniline; In acetic acid; propionic acid; at 0 ℃;

With sodium nitrite; In acetic acid; propionic acid; for 1h;
DOI:10.1002/chem.201400114

Reference yield:

: 118788-67-3
N-(4-decyl-2-nitrophenyl)acetamide

: 1598408-16-2
2-nitro-4-decyldiazobenzene tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / acetic acid / 2 h / 80 °C

2.1: acetic acid; propionic acid / 0 °C

2.2: 1 h

With hydrogenchloride; In acetic acid; propionic acid;
DOI:10.1002/chem.201400114

Reference yield:

: 37529-30-9
4-n-decylaniline

: 1598408-16-2
2-nitro-4-decyldiazobenzene tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(II) nitrate trihydrate / acetic acid / 1 h

2.1: hydrogenchloride / acetic acid / 2 h / 80 °C

3.1: acetic acid; propionic acid / 0 °C

3.2: 1 h

With hydrogenchloride; copper(II) nitrate trihydrate; In acetic acid; propionic acid;
DOI:10.1002/chem.201400114