1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

Base Information

Chemical Name:1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene
CAS No.:150919-07-6
Molecular Formula:C₁₃₂H₁₆₈O₈
Molecular Weight:1882.78
Hs Code.:

Synonyms:1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

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Chemical Property of 1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

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Technology Process of 1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

There total 3 articles about 1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

: p-tert-butylcalix[8]arene trianion tetraethylammonium salt

: 150919-07-6
1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

: 5,11,17,23,29,35,41,47-octa-tert-butyl-49-[(4-tert-butylbenzyl)oxy]calix[8]arene-50,51,52,53,54,55,56-heptol

: 5,11,17,23,29,35,41,47-octa-tert-butyl-49,51-bis[(4-tert-butylbenzyl)oxy]calix[8]arene-50,52,53,54,55,56-hexol

: C₁₂₁H₁₅₄O₈

Guidance literature:: In tetrahydrofuran; N,N-dimethyl-formamide; Further byproducts given; Heating;
DOI:10.1021/jo970029u

Reference yield: 25.0%

: 18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

: p-tert-butylcalix[8]arene trianion tetraethylammonium salt

: 150919-07-6
1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

: 5,11,17,23,29,35,41,47-octa-tert-butyl-49-[(4-tert-butylbenzyl)oxy]calix[8]arene-50,51,52,53,54,55,56-heptol

: 5,11,17,23,29,35,41,47-octa-tert-butyl-49,51-bis[(4-tert-butylbenzyl)oxy]calix[8]arene-50,52,53,54,55,56-hexol

: C₁₂₁H₁₅₄O₈

Guidance literature:: In tetrahydrofuran; N,N-dimethyl-formamide; Further byproducts given; Heating;
DOI:10.1021/jo970029u

Reference yield:

: 68971-82-4,106750-70-3,78092-52-1
5,11,17,23,29,35,41,47-octakis(tert-butyl)-49,50,51,52,53,54,55,56-octakis(hydroxy)calix[8]arene

: 18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

: 150919-07-6
1,3,5,7-tetrakis(p-tert-butylbenzyl) ether of p-tert-butylcalix[8]arene

Guidance literature:: With potassium carbonate; Yield given. Multistep reaction; 1.) THF, DMF, 60 deg C, 20 min, 2.) THF, 60 deg C, 20 h;
DOI:10.1016/S0040-4039(00)73693-8