trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

Base Information

Chemical Name:trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester
CAS No.:1604803-34-0
Molecular Formula:C₂₁H₂₁ClF₃N₃O₇
Molecular Weight:519.862
Hs Code.:

Synonyms:trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

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Chemical Property of trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

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Technology Process of trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

There total 5 articles about trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1604803-33-9
{4-[2-(4-chloro-2-methoxypyridin-3-yl)-2-hydroxyethyl]-3-nitrophenyl}carbamic acid tert-butyl ester

: 407-25-0
trifluoroacetic anhydride

: 1604803-34-0
trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 0.5h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1604803-34-0
trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-aminopyridine / tetrahydrofuran / 3 h / 25 °C

2.1: tetrahydrofuran / 1 h / -70 °C / Inert atmosphere

2.2: 1 h / -70 - 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C

4.1: tetrahydrofuran / 0.5 h / 25 °C

With 4-aminopyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;

Reference yield:

: 99-09-2
3-nitro-aniline

: 1604803-34-0
trifluoroacetic acid 2-(4-tert-butoxycarbonylamino-2-nitrophenyl)-1-(4-chloro-2-methoxypyridin-3-yl)ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-aminopyridine / tetrahydrofuran / 3 h / 25 °C

2.1: tetrahydrofuran / 1 h / -70 °C / Inert atmosphere

2.2: 1 h / -70 - 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C

4.1: tetrahydrofuran / 0.5 h / 25 °C

With 4-aminopyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;