(2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide

Base Information

Chemical Name:(2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide
CAS No.:1068602-15-2
Molecular Formula:C₂₇H₄₇NO₃Si
Molecular Weight:461.761
Hs Code.:

Synonyms:(2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide

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Technology Process of (2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide

There total 1 articles about (2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1185862-06-9
C₁₀H₂₃LiOSi

: 1068601-67-1,38735-14-7
N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylmethacrylamide

: 106-95-6
allyl bromide

: (2S,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide

: 1068602-15-2
(2R,5S)-2-allyl-6-(tert-butyldimethylsilyloxy)-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2,5-trimethylhexanamide

Guidance literature:: N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylmethacrylamide; With methyllithium; lithium chloride; In tetrahydrofuran; formaldehyde diethyl acetal; at -78 ℃; Inert atmosphere;

C₁₀H₂₃LiOSi; In tetrahydrofuran; diethyl ether; formaldehyde diethyl acetal; pentane; at -78 - -40 ℃; Inert atmosphere;

allyl bromide; In tetrahydrofuran; diethyl ether; formaldehyde diethyl acetal; pentane; at -40 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja806021y