3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

Base Information

Chemical Name:3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate
CAS No.:1414124-86-9
Molecular Formula:C₂₆H₃₇F₃O₇S
Molecular Weight:550.637
Hs Code.:

Synonyms:3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

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Chemical Property of 3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

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Technology Process of 3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

There total 4 articles about 3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1414124-71-2
1,3-bis(methoxymethoxy)-5-{[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]oxy}benzene

: 1414124-86-9
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

Guidance literature:: 1,3-bis(methoxymethoxy)-5-{[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]oxy}benzene; With pyridine; In dichloromethane; at -20 ℃; for 0.5h; Inert atmosphere;

trifluoromethylsulfonic anhydride; In dichloromethane; at -20 ℃; for 2h;
DOI:10.1055/s-0032-1316765

Reference yield:

: 1414124-56-3
1,3-bis(methoxymethoxy)-5-{[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]oxy}benzene

: 1414124-86-9
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-aniline / 3 h / 200 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 0.5 h / -20 °C / Inert atmosphere

2.2: 2 h / -20 °C

With pyridine; In dichloromethane; N,N-dimethyl-aniline; 1.1: |Claisen Rearrangement;
DOI:10.1055/s-0032-1316765

Reference yield:

: 3,5-bis(methoxymethyl)phloroglucinol

: 1414124-86-9
3,5-bis(methoxymethoxy)-4-[(2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienyl]phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

2.1: N,N-dimethyl-aniline / 3 h / 200 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 0.5 h / -20 °C / Inert atmosphere

3.2: 2 h / -20 °C

With pyridine; potassium carbonate; In dichloromethane; N,N-dimethyl-aniline; N,N-dimethyl-formamide; 2.1: |Claisen Rearrangement;
DOI:10.1055/s-0032-1316765