dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

Base Information

Chemical Name:dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate
CAS No.:1293917-96-0
Molecular Formula:C₁₃H₁₄FO₅P
Molecular Weight:300.223
Hs Code.:

Synonyms:dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

Suppliers and Price of dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

There total 2 articles about dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 59414-23-2
1-methoxy-3-<(trimethylsilyl)oxy>01,3-butadiene

: 141543-24-0
Dimethyl 2-fluorobenzoylphosphonate

: 1293917-96-0
dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

Guidance literature:: 1-methoxy-3-<(trimethylsilyl)oxy>01,3-butadiene; Dimethyl 2-fluorobenzoylphosphonate; In toluene; at 100 ℃; for 6h; Inert atmosphere;

With trifluoroacetic acid; In toluene; at 0 ℃;
DOI:10.1016/j.tet.2011.02.007

Reference yield:

: 393-52-2
2-Fluorobenzoyl chloride

: 1293917-96-0
dimethyl (2-(2-fluorophenyl)-4-oxo-3,4-dihydro-2H-pyran-2-yl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 0 °C

2.1: toluene / 6 h / 100 °C / Inert atmosphere

2.2: 0 °C

In toluene; 1.1: Michaelis-Arbuzov reaction / 2.1: Diels-Alder reaction;
DOI:10.1016/j.tet.2011.02.007