bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

Base Information

Chemical Name:bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide
CAS No.:863551-41-1
Molecular Formula:C₇₈H₁₃₄S₆Si₁₂
Molecular Weight:1601.34
Hs Code.:

Synonyms:bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

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Chemical Property of bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

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Technology Process of bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

There total 5 articles about bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 863551-62-6
2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylthio}iodobenzene

: 17534-15-5
Benzene-1,2-dithiol

: 863551-41-1
bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

Guidance literature:: With copper(I) oxide; In 2,4,6-trimethyl-pyridine; for 3h; Heating;
DOI:10.1016/j.jorganchem.2006.10.056

Reference yield:

: 2-{2-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenylsulfanyl]-phenylsulfanyl}-benzenethiol

: 863551-41-1
bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

Guidance literature:: With iodine;
DOI:10.1080/10426500590911421

Reference yield:

: HS(2,4,6-((SiMe₃)2CH)3C₆H₂)

: 863551-41-1
bis[2-(2-{2,4,6-tris[bis(trimethylsilyl)methyl]phenylsulfanyl}phenylsulfanyl)phenyl]disulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / Cu₂O; 2,4,6-trimethylpyridine / 3 h / Heating

2: 52 percent / Cu₂O; 2,4,6-trimethylpyridine / 3 h / Heating

3: 1.50 g / air / 12 h / 20 °C

With 2,4,6-trimethyl-pyridine; copper(I) oxide; air;
DOI:10.1039/b513339d