2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

Base Information

Chemical Name:2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid
CAS No.:131262-37-8
Molecular Formula:C₁₁H₁₀F₂O₂
Molecular Weight:212.196
Hs Code.:

Synonyms:2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

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Chemical Property of 2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

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Technology Process of 2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

There total 4 articles about 2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 131262-28-7
1,1-Difluoro-r-3-hydroxymethyl-cis-2-methyl-trans-2-phenylcyclopropane

: 131262-37-8
2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

Guidance literature:: With sodium hydroxide; potassium permanganate; In water; at -10 ℃; for 1h;
DOI:10.1016/S0040-4020(01)87829-7

Reference yield:

: 54976-38-4
(E)-3-phenylbut-2-en-1-ol

: 131262-37-8
2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / 25 °C

2: 76 percent / 10 h

3: 85 percent / p-toluenesulfonic acid, glycerine / up to 100 deg C

4: 92 percent / KMnO₄, NaOH / H₂O / 1 h / -10 °C

With sodium hydroxide; potassium permanganate; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; glycerol; In dichloromethane; water;
DOI:10.1016/S0040-4020(01)87829-7

Reference yield:

: 131262-21-0
2-[(E)-3-phenyl-2-butenyloxy]-tetrahydro-2H-pyran

: 131262-37-8
2,2-Difluoro-cis-3-methyl-trans-3-phenyl-r-1-cyclopropanecarboxylic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 10 h

2: 85 percent / p-toluenesulfonic acid, glycerine / up to 100 deg C

3: 92 percent / KMnO₄, NaOH / H₂O / 1 h / -10 °C

With sodium hydroxide; potassium permanganate; toluene-4-sulfonic acid; glycerol; In water;
DOI:10.1016/S0040-4020(01)87829-7