(S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

Base Information

Chemical Name:(S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid
CAS No.:1352824-59-9
Molecular Formula:C₂₂H₂₂N₂O₇
Molecular Weight:426.426
Hs Code.:

Synonyms:(S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

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Chemical Property of (S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

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Technology Process of (S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

There total 5 articles about (S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1352824-60-2
C₂₃H₂₄N₂O₇

: 1352824-59-9
(S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

Guidance literature:: C₂₃H₂₄N₂O₇; With ethanol; sodium hydroxide; at 80 ℃; for 1h; Sealed tube;

With hydrogenchloride; In ethanol; water; pH=3;

Reference yield:

: 10242-08-7
5-methoxybenzofuran-2-carboxylic acid

: 1352824-59-9
(S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / Reflux

2.1: triethylamine / dichloromethane / 20 °C

3.1: sodium hydroxide; ethanol / 1 h / 80 °C / Sealed tube

3.2: pH 3

With thionyl chloride; ethanol; triethylamine; sodium hydroxide; In dichloromethane;

Reference yield:

: 23680-31-1
BOC-O-benzyl-L-serine

: 1352824-59-9
(S)-2-(3-(benzyloxy)-2-(5-methoxybenzofuran-2-carboxamido)propanamido)acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

3.1: triethylamine / dichloromethane / 20 °C

4.1: sodium hydroxide; ethanol / 1 h / 80 °C / Sealed tube

4.2: pH 3

With ethanol; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;