Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

Base Information

Chemical Name:Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester
CAS No.:147623-22-1
Molecular Formula:C₁₈H₂₀BrNO₅S
Molecular Weight:442.331
Hs Code.:

Synonyms:Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

Suppliers and Price of Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

There total 1 articles about Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 98-59-9
p-toluenesulfonyl chloride

: Acetic acid 3-amino-2-bromo-6-methoxy-4,5-dimethyl-phenyl ester

: 147623-22-1
Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

Guidance literature:: With pyridine; In dichloromethane; for 96h;
DOI:10.1021/jo00061a017

Reference yield: 97.0%

: 147623-28-7
(3-Bromo-cyclohex-1-enesulfonyl)-benzene

: 147623-22-1
Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

: 148163-39-7,148219-16-3
N-(3-Acetoxy-2-bromo-4-methoxy-5,6-dimethylphenyl)-N-<(3-phenylsulfonyl)-2-cyclohexenyl>-4-methylbenzenesulfonamide

Guidance literature:: With potassium carbonate; In acetone; for 18h; Heating;
DOI:10.1021/jo00061a017

Reference yield:

: 147623-22-1
Acetic acid 2-bromo-6-methoxy-4,5-dimethyl-3-(toluene-4-sulfonylamino)-phenyl ester

: N-(5-Benzyloxy-4-methoxy-2,3-dimethyl-phenyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

2: KOH / ethanol

3: 94 percent / aq. NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 16 h

4: Ph₃SnH, AIBN / benzene / 6 h / Heating

With potassium hydroxide; sodium hydroxide; 2,2'-azobis(isobutyronitrile); triphenylstannane; tetrabutylammomium bromide; In ethanol; dichloromethane; benzene;
DOI:10.1021/jo00061a017