2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

Base Information

Chemical Name:2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure
CAS No.:156417-84-4
Molecular Formula:C₃₄H₃₀N₂O₁₂S₂
Molecular Weight:722.75
Hs Code.:

Synonyms:2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

Suppliers and Price of 2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

There total 1 articles about 2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 140410-13-5
5,7,14,16-tetrakis(ethoxycarbonyl)-2,11-bis(4-tolylsulfonyl)-2,11-diaza<3.3>metacyclophane

: 156417-84-4
2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

Guidance literature:: With potassium hydroxide; In ethanol; for 2h; Heating;

Reference yield:

: 156417-84-4
2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

: C-[8,14,16-Tris-aminomethyl-3,11-bis-(toluene-4-sulfonyl)-3,11-diaza-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁶⁾,5⁽¹⁸⁾,6,8,13⁽¹⁷⁾,14-hexaen-6-yl]-methylamine

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂, DMF / Heating

2: NH₃ / dioxane / 1 h / <30 deg C

3: 1M diborane / tetrahydrofuran / 8 h / Heating

With thionyl chloride; ammonia; N,N-dimethyl-formamide; diborane; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 156417-84-4
2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarbonsaeure

: 156417-85-5
2,11-Bis(p-tolylsulfonyl)-2,11-diaza<3.3>metacyclophan-5,7,14,16-tetracarboxamid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / Heating

2: NH₃ / dioxane / 1 h / <30 deg C

With thionyl chloride; ammonia; N,N-dimethyl-formamide; In 1,4-dioxane;