(3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

Base Information

Chemical Name:(3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane
CAS No.:943032-35-7
Molecular Formula:C₂₁H₂₉NO₄
Molecular Weight:359.466
Hs Code.:

Synonyms:(3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

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Chemical Property of (3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

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Technology Process of (3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

There total 4 articles about (3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 745809-24-9
C₁₄H₂₀O₄

: 943032-35-7
(3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 69 percent / KMnO₄; MgSO₄ / RuCl₃ / H₂O; ethanol / 2 h / 20 °C / pH 7

2.1: NaIO₄ / methanol

2.2: aq. NaHCO₃ / ethyl acetate

3.1: NaBH(OAc)3 / CH₂Cl₂ / 20 °C

With potassium permanganate; sodium periodate; sodium tris(acetoxy)borohydride; magnesium sulfate; ruthenium trichloride; In methanol; ethanol; dichloromethane; water;
DOI:10.1021/jo070058x

Reference yield:

: 848837-64-9
C₁₄H₂₂O₆

: 100-46-9
benzylamine

: 943032-35-7
(3S,4R,6R)-6-O-acetyl-1-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

: 943032-38-0
(3R,4R,5R)-1-benzyl-3-O-acetyl-4,5-O-cyclohexylidene-3,4,5-trihydroxyazepane

Guidance literature:: C₁₄H₂₂O₆; With sodium periodate; In methanol;

With sodium hydrogencarbonate; In ethyl acetate;

benzylamine; With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; Further stages.;
DOI:10.1021/jo070058x