(+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine

Base Information

• Chemical Name: (+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine
• CAS No.: 139561-03-8
• Molecular Formula: C₁₉H₂₇NO₇
• Molecular Weight: 381.426

Synonyms:(+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine

Chemical Property of (+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine

Chemical Property:

Purity/Quality:

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Technology Process of (+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine

There total 25 articles about (+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine (139461-80-6,139461-81-7,139561-01-6,139561-02-7,139561-03-8,139561-04-9) → (+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine (139561-03-8)

Guidance literature:

In hexane; for 6h; Ambient temperature;

DOI:10.1021/jm00086a009

Reference yield: 90.0%

N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(E)-2,3-methano-m-tyrosine ethyl ester (139461-76-0,139461-77-1) → N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(E)-2,3-methano-m-tyrosine (139461-80-6,139461-81-7,139561-01-6,139561-02-7,139561-03-8,139561-04-9)

Guidance literature:

With sodium hydroxide; In ethanol; Heating;

DOI:10.1021/jm00086a009

Reference yield: 85.0%

N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine methyl ester → N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine (139461-80-6,139461-81-7,139561-01-6,139561-02-7,139561-03-8,139561-04-9)

Guidance literature:

With sodium hydroxide; In ethanol; Ambient temperature;

DOI:10.1021/jm00086a009

upstream raw materials:

N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(Z)-2,3-methano-m-tyrosine

meta-hydroxybenzaldehyde

(3-methoxyethoxymethyloxy)benzaldehyde

diethyl <3-<(2-methoxyethoxy)methoxy>benzal>malonate

Downstream raw materials:

(+)-(Z)-2,3-methano-m-tyrosine

(+)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(E)-2,3-methano-m-tyrosine

(-)-N-<(1,1-dimethylethoxy)carbonyl>-O-<(2-methoxyethoxy)methyl>-(E)-2,3-methano-m-tyrosine

(E)-2,3-methano-m-tyrosine hydrochloride

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