(S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

Base Information

Chemical Name:(S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine
CAS No.:147912-84-3
Molecular Formula:C₂₈H₂₂BrNO₂
Molecular Weight:484.392
Hs Code.:

Synonyms:(S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

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Chemical Property of (S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

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Technology Process of (S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

There total 1 articles about (S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42538-40-9
(S)-2-amino-3-(2-bromophenyl)propanoic acid

: 55135-66-5
9-bromo-9-phenyl-9H-fluorene

: 147912-84-3
(S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

Guidance literature:: With chloro-trimethyl-silane; lead(II) nitrate; triethylamine; Yield given. Multistep reaction; 1.) CHCl₃, 2 h, reflux, 2.) CHCl₃, r.t., 4 d;
DOI:10.1021/jo00062a018

Reference yield: 90.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 147912-84-3
(S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

: 147976-11-2
(S)-3-(9-phenylfluoren-9-yl)-4-<(2-bromophenyl)methyl>oxazolidin-5-one

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; water; Ambient temperature;
DOI:10.1021/jo00062a018

Reference yield:

: 147912-84-3
(S)-N-(9-phenylfluoren-9-yl)-o-bromophenylalanine

: (S)-2-indan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / p-toluenesulfonic acid monohydrate / H₂O; tetrahydrofuran / Ambient temperature

2: 98 percent / 1.) n-BuLi, 2.) AcOH / multistep reaction; other oxazolidinones, enantioselectivity

With n-butyllithium; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; water;
DOI:10.1021/jo00062a018