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Technology Process of (C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

Base Information
  • Chemical Name:(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I
  • CAS No.:865876-19-3
  • Molecular Formula:C137H122BF2IN12O12
  • Molecular Weight:2304.26
  • Hs Code.:
(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2(CCC<sub>6</sub>H<sub>4</sub>)3C(CC(CH<sub>3</sub>)C(C<sub>2</sub>H<sub>5</sub>)CCH<sub>3</sub>N)2BF<sub>2</sub>))C<sub>6</sub>H<sub>13</sub>CHC<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>8</sub>H<sub>8</sub>I

Synonyms:(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

Suppliers and Price of (C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I
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Chemical Property of (C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I
Chemical Property:
Purity/Quality:

98% *data from raw suppliers

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Useful:
Technology Process of (C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

There total 3 articles about (C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

(3-ethyl-5-((4-ethyl-3,5-dimethyl-2H-pyrrol-2-ylidene-κN)-[4-((4-[(4-ethynylphenyl)ethynyl]phenyl)ethynyl)phenyl]methyl)-2,4-dimethyl-1H-pyrrolato-κN)(difluoro)boron

(3-ethyl-5-((4-ethyl-3,5-dimethyl-2H-pyrrol-2-ylidene-κN)-[4-((4-[(4-ethynylphenyl)ethynyl]phenyl)ethynyl)phenyl]methyl)-2,4-dimethyl-1H-pyrrolato-κN)(difluoro)boron

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNCC(O)N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2I)C(O)CNCO))2

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2OCNCC(O)N(C6H2(CH3)2I)C(O)CNCO))2

(C<sub>6</sub>H<sub>2</sub>O<sub>2</sub>CH(C<sub>6</sub>H<sub>13</sub>))4(C<sub>8</sub>N<sub>2</sub>H<sub>4</sub>)2(C<sub>6</sub>N<sub>3</sub>(O)2C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2(CCC<sub>6</sub>H<sub>4</sub>)3C(C<sub>4</sub>N(CH<sub>3</sub>)2C<sub>2</sub>H<sub>5</sub>)2BF<sub>2</sub>)2

(C6H2O2CH(C6H13))4(C8N2H4)2(C6N3(O)2C6H2(CH3)2(CCC6H4)3C(C4N(CH3)2C2H5)2BF2)2

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2(CCC<sub>6</sub>H<sub>4</sub>)3C(CC(CH<sub>3</sub>)C(C<sub>2</sub>H<sub>5</sub>)CCH<sub>3</sub>N)2BF<sub>2</sub>))C<sub>6</sub>H<sub>13</sub>CHC<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>8</sub>H<sub>8</sub>I
865876-19-3

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

Guidance literature:
With copper(l) iodide; In tetrahydrofuran; 0.75 equiv. of B compd.; 35°C, 2 d; sepd. by gel permeation chromy. (CH2Cl2);
DOI:10.1002/anie.200500970

Reference yield: 28.0%

(3-ethyl-5-((4-ethyl-3,5-dimethyl-2H-pyrrol-2-ylidene-κN)-[4-((4-[(4-ethynylphenyl)ethynyl]phenyl)ethynyl)phenyl]methyl)-2,4-dimethyl-1H-pyrrolato-κN)(difluoro)boron

(3-ethyl-5-((4-ethyl-3,5-dimethyl-2H-pyrrol-2-ylidene-κN)-[4-((4-[(4-ethynylphenyl)ethynyl]phenyl)ethynyl)phenyl]methyl)-2,4-dimethyl-1H-pyrrolato-κN)(difluoro)boron

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNCC(O)N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2I)C(O)CNCO))2

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2OCNCC(O)N(C6H2(CH3)2I)C(O)CNCO))2

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2(CCC<sub>6</sub>H<sub>4</sub>)3C(CC(CH<sub>3</sub>)C(C<sub>2</sub>H<sub>5</sub>)CCH<sub>3</sub>N)2BF<sub>2</sub>))C<sub>6</sub>H<sub>13</sub>CHC<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>8</sub>H<sub>8</sub>I
865876-19-3

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2(CCC<sub>6</sub>H<sub>4</sub>)3C(CC(CH<sub>3</sub>)C(C<sub>2</sub>H<sub>5</sub>)CCH<sub>3</sub>N)2BF<sub>2</sub>))2

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))2

Guidance literature:
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; chromd. (SiO2); chromd. (gel);
DOI:10.1246/bcsj.79.1926

Reference yield: 26.0%

(3-ethyl-5-((4-ethyl-3,5-dimethyl-2H-pyrrol-2-ylidene-κN)-[4-((4-[(4-ethynylphenyl)ethynyl]phenyl)ethynyl)phenyl]methyl)-2,4-dimethyl-1H-pyrrolato-κN)(difluoro)boron

(3-ethyl-5-((4-ethyl-3,5-dimethyl-2H-pyrrol-2-ylidene-κN)-[4-((4-[(4-ethynylphenyl)ethynyl]phenyl)ethynyl)phenyl]methyl)-2,4-dimethyl-1H-pyrrolato-κN)(difluoro)boron

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNCC(O)N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2I)C(O)CNCO))2

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2OCNCC(O)N(C6H2(CH3)2I)C(O)CNCO))2

(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>OCNC<sub>6</sub>H<sub>4</sub>NCO))2(C<sub>6</sub>H<sub>13</sub>CH(C<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)2(CCC<sub>6</sub>H<sub>4</sub>)3C(CC(CH<sub>3</sub>)C(C<sub>2</sub>H<sub>5</sub>)CCH<sub>3</sub>N)2BF<sub>2</sub>))C<sub>6</sub>H<sub>13</sub>CHC<sub>6</sub>H<sub>2</sub>O<sub>2</sub>C<sub>6</sub>O<sub>2</sub>N<sub>3</sub>C<sub>8</sub>H<sub>8</sub>I
865876-19-3

(C6H13CH(C6H2OCNC6H4NCO))2(C6H13CH(C6H2O2C6O2N3C6H2(CH3)2(CCC6H4)3C(CC(CH3)C(C2H5)CCH3N)2BF2))C6H13CHC6H2O2C6O2N3C8H8I

Guidance literature:
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 23 ℃; Inert atmosphere;
DOI:10.1002/chem.201001625
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