furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

Base Information

Chemical Name:furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride
CAS No.:1091681-89-8
Molecular Formula:C₁₈H₂₂N₂O₃*ClH
Molecular Weight:350.845
Hs Code.:

Synonyms:furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

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Chemical Property of furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

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Technology Process of furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

There total 3 articles about furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 1091681-89-8
furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

2: sodium hydroxide / water; tetrahydrofuran / 20 °C

3: hydrogenchloride / water; ethyl acetate / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2016.04.086

Reference yield:

: 883516-51-6
4-[(furan-2-ylmethyl)amino]piperidin-1-carboxylic acid tert-butyl ester

: 1091681-89-8
furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; tetrahydrofuran / 20 °C

2: hydrogenchloride / water; ethyl acetate / 20 °C

With hydrogenchloride; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.bmcl.2016.04.086

Reference yield:

: 87120-72-7
1-(tert-butoxycarbonyl)-4-aminopiperidine

: 1091681-89-8
furan-2-ylmethyl-piperidin-4-yl-carbamic acid benzyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

2: sodium hydroxide / water; tetrahydrofuran / 20 °C

3: hydrogenchloride / water; ethyl acetate / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; sodium hydroxide; In tetrahydrofuran; water; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2016.04.086