Technology Process of C34H60N5O9PS
There total 11 articles about C34H60N5O9PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
acetone;
for 36h;
Reflux;
Inert atmosphere;
DOI:10.1039/c1ob05384a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetonitrile / 1 h / Inert atmosphere
2.1: trimethylphosphane / tetrahydrofuran / 4 h / Inert atmosphere
2.2: 0.5 h
3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere
4.1: sodium iodide / acetone / 36 h / Reflux; Inert atmosphere
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium iodide; trimethylphosphane;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c1ob05384a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -40 °C / Inert atmosphere
3.1: acetonitrile / 1 h / Inert atmosphere
4.1: trimethylphosphane / tetrahydrofuran / 4 h / Inert atmosphere
4.2: 0.5 h
5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere
6.1: sodium iodide / acetone / 36 h / Reflux; Inert atmosphere
With
2,6-dimethylpyridine; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium iodide; trimethylphosphane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c1ob05384a
