1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

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Chemical Name:1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane
CAS No.:227959-02-6
Molecular Formula:C₇₈H₉₆O₁₆Si
Molecular Weight:1317.7
Hs Code.:

1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

Synonyms:1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

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Chemical Property of 1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

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Technology Process of 1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

There total 9 articles about 1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy tosylate

: 1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-hydroxyphenoxy}-3,6,9-trioxaundecane

: 227959-02-6
1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1039/a900914k

Reference yield:

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 227959-02-6
1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaH / tetrahydrofuran / 3 h / Heating

2: 36 percent / NaH / tetrahydrofuran / 2 h / Heating

With sodium hydride; In tetrahydrofuran;
DOI:10.1021/ma034521t

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 227959-02-6
1-{p-[2-(2-(2-(2-(diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-13-{p-[2-(2-(2-(2-(4-((diphenyl-tert-butyl)siloxy)diphenylmethoxy)ethoxy)ethoxy)ethoxy)ethoxy]phenoxy}-3,6,9-trioxaundecane

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / pyridine; Et₃N; DMAP / CH₂Cl₂ / 5 h / 20 °C

2: 79 percent / NaBH₄ / tetrahydrofuran / 7 h / Heating

3: 65 percent / NaH / tetrahydrofuran / 3 h / Heating

4: 36 percent / NaH / tetrahydrofuran / 2 h / Heating

With pyridine; dmap; sodium tetrahydroborate; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ma034521t