3',5'-diisovalerylacetophenone

Base Information

• Chemical Name: 3',5'-diisovalerylacetophenone
• CAS No.: 406919-42-4
• Molecular Formula: C₁₈H₂₄O₅
• Molecular Weight: 320.386
• Mol file: 406919-42-4.mol

Synonyms:3',5'-diisovalerylacetophenone

Chemical Property of 3',5'-diisovalerylacetophenone

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3',5'-diisovalerylacetophenone

There total 1 articles about 3',5'-diisovalerylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

3,5-dihydroxyacetophenone (51863-60-6) + isopentanoyl chloride (108-12-3) → 3',5'-diisovalerylacetophenone (406919-42-4)

Guidance literature:

With pyridine; at 20 ℃;

DOI:10.1002/jps.1055

Reference yield: 74.0%

3',5'-diisovalerylacetophenone (406919-42-4) → 2-bromo-3',5'-diisovaleryloxyacetophenone (406919-46-8)

Guidance literature:

With pyridinium bromide perbromate; In acetic acid; at 20 ℃; for 1h;

DOI:10.1002/jps.1055

Reference yield:

3',5'-diisovalerylacetophenone (406919-42-4) → 2-tert-butylamino-3',5'-diisovaleryloxyacetophenone hydrochloride

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / pyridinium bromide perbromate / acetic acid / 1 h / 20 °C

2: 24 percent / HCl / CH₂Cl₂ / 1 h

With hydrogenchloride; pyridinium bromide perbromate; In dichloromethane; acetic acid;

DOI:10.1002/jps.1055

upstream raw materials:

3,5-dihydroxyacetophenone

isopentanoyl chloride

Downstream raw materials:

2-bromo-3',5'-diisovaleryloxyacetophenone