(2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

Base Information

Chemical Name:(2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid
CAS No.:1356919-28-2
Molecular Formula:C₂₄H₂₀ClN₃O₅S
Molecular Weight:497.959
Hs Code.:

Synonyms:(2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

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Chemical Property of (2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

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Technology Process of (2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

There total 4 articles about (2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-{(3S)-4-[(4S)-4-benzyl-2-oxo-1,3-thiazolidin-3-yl]-3-[(S)-{4-[(4-chlorophenyl)sulfanyl]phenyl}(hydroxy)methyl]-4-oxobutyl}-1,2,3-benzotriazin-4(3H)-one

: 1356919-28-2
(2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

Guidance literature:: With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1356919-28-2
(2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

2.1: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.75 h / 0 °C / Inert atmosphere

2.3: 5 h / 0 - 20 °C / Inert atmosphere

3.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With dihydrogen peroxide; titanium tetrachloride; potassium carbonate; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 1356919-28-2
(2S)-2-[(S)-{4-[(4-chlorophenyl)sulfinyl]phenyl}(hydroxy)methyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

2.1: titanium tetrachloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.75 h / 0 °C / Inert atmosphere

2.3: 5 h / 0 - 20 °C / Inert atmosphere

3.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With dihydrogen peroxide; titanium tetrachloride; potassium carbonate; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;