N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

Base Information

Chemical Name:N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate
CAS No.:1323443-53-3
Molecular Formula:C₂HF₃O₂*C₄₇H₈₄N₂O₃S₂
Molecular Weight:903.352
Hs Code.:

Synonyms:N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

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Chemical Property of N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

Chemical Property:

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Technology Process of N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

There total 5 articles about N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1323443-51-1
[2-(2-{[3,4-di(oleyloxy)benzoyl]amino}-ethyldisulfanyl)ethyl]-carbamic acid tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 1323443-53-3
N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

Guidance literature:: Inert atmosphere; Cooling with ice;
DOI:10.1016/j.bbamem.2011.04.020

Reference yield:

: 926652-62-2
3,4-bis-octadec-9-enyloxy-benzoic acid ethyl ester

: 1323443-53-3
N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; potassium hydroxide / 4 h / Inert atmosphere; Reflux

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / Inert atmosphere

3: Inert atmosphere; Cooling with ice

With ethanol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In dichloromethane;
DOI:10.1016/j.bbamem.2011.04.020

Reference yield:

: 143-28-2,593-47-5,84286-21-5
oleoyl alcohol

: 1323443-53-3
N-[2-(2-aminoethyldisulfanyl)-ethyl]-3,4-di(oleyloxy)benzamide trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 5 - 50 °C

2: ethanol; potassium hydroxide / 4 h / Inert atmosphere; Reflux

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / Inert atmosphere

4: Inert atmosphere; Cooling with ice

With ethanol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; potassium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene; 1: Mitsunobu reaction;
DOI:10.1016/j.bbamem.2011.04.020