ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

Base Information

Chemical Name:ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate
CAS No.:1300748-88-2
Molecular Formula:C₁₉H₂₀N₂O₄
Molecular Weight:340.379
Hs Code.:

Synonyms:ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

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Technology Process of ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

There total 4 articles about ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: C₁₃H₁₄N₂O

: 26367-48-6
fumaric acid ethyl ester mono chloride

: 1300748-88-2
ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: methyl 3-(1-benzylimidazol-4-yl)-2-propenoate

: 1300748-88-2
ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With diisobutylaluminium hydride; triethylamine; In dichloromethane;
DOI:10.1039/c0ob00657b

Reference yield:

: 104-98-3
urocanic acid

: 1300748-88-2
ethyl (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (2E)-2-butenedioate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; magnesium sulfate / Reflux

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride

4: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; diisobutylaluminium hydride; magnesium sulfate; triethylamine; In tetrahydrofuran; dichloromethane; 1: Fischer esterification;
DOI:10.1039/c0ob00657b