13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene

Base Information

Chemical Name:13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene
CAS No.:122372-62-7
Molecular Formula:C₁₆H₂₂O₈S
Molecular Weight:374.412
Hs Code.:

Synonyms:13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene

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Technology Process of 13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene

There total 2 articles about 13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1822-66-8
3,4-dihydroxythiophene-2,5-dicarboxylic acid diethyl ester

: 112-27-6
2,2'-[1,2-ethanediylbis(oxy)]bisethanol

: 122372-62-7
13,15-bis(ethoxycarbonyl)-2,5,8,11-tetraoxa-14-thiabicyclo<10.3.0>pentadeca-1(15),12-diene

Guidance literature:: With tributylphosphine; diamide; In tetrahydrofuran; at 60 ℃; Darkness; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.03.062