phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

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Chemical Name:phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate
CAS No.:897019-43-1
Molecular Formula:C₂₁H₁₈ClN₅O₃
Molecular Weight:423.859
Hs Code.:

Synonyms:phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

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Chemical Property of phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

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Technology Process of phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

There total 3 articles about phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 897019-38-4
allyl (3-(4-chlorophenyl)-4,5-dihydro-1H-pyrazol-4-yl)-carbamate

: 79463-77-7
N-cyanodiphenylcarbonimidate

: 897019-43-1
phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

Guidance literature:: In isopropyl alcohol; for 1h; Heating / reflux;

Reference yield:

: C₁₈H₂₃ClN₂O₃

: 897019-43-1
phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / Reflux

2: isopropyl alcohol / 1 h / Reflux

With hydrazine hydrate; In ethanol; isopropyl alcohol;
DOI:10.1021/acs.jmedchem.5b01890

Reference yield:

: 178888-24-9
allyl (2-(4-chlorophenyl)-2-oxoethyl)-carbamate

: 897019-43-1
phenyl 4-allyloxycarbonylamino-3-(4-chlorophenyl)-N-cyano-4,5-dihydro-1H-pyrazol-1-carboximidoate

Guidance literature:: Multi-step reaction with 3 steps

1: water; ethanol / 20 °C

2: hydrazine hydrate / ethanol / Reflux

3: isopropyl alcohol / 1 h / Reflux

With hydrazine hydrate; In ethanol; water; isopropyl alcohol; 1: |Mannich Aminomethylation;
DOI:10.1021/acs.jmedchem.5b01890