allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Base Information

Chemical Name:allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate
CAS No.:113599-71-6
Molecular Formula:C₃₀H₂₉ClN₂O₅
Molecular Weight:533.024
Hs Code.:

Synonyms:allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Suppliers and Price of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

There total 6 articles about allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 113599-64-7
allyl 2-<(3S,4S)-4-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

: 113599-71-6
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.25h;
DOI:10.1021/jm00401a020

Reference yield:

: 40630-84-0
allyl bromoacetate

: 113599-71-6
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent

2: LiN(SiMe₃)2 / tetrahydrofuran / -78 °C

3: tetrabutylammonium fluoride, HOAc / tetrahydrofuran

With tetrabutyl ammonium fluoride; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1039/c39870001283

Reference yield:

: 113599-63-6
allyl 2-<(3S,4S)-4-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxo-3-(tritylamino)-1-azetidinyl>acetate

: 113599-71-6
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-4-chlorobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: LiN(SiMe₃)2 / tetrahydrofuran / -78 °C

2: tetrabutylammonium fluoride, HOAc / tetrahydrofuran

With tetrabutyl ammonium fluoride; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1039/c39870001283