9-(Chlorodiphenylsilyl)-9H-fluorene

Base Information

Chemical Name:9-(Chlorodiphenylsilyl)-9H-fluorene
CAS No.:73220-53-8
Molecular Formula:C25H19ClSi
Molecular Weight:382.96
Hs Code.:
DSSTox Substance ID:DTXSID70376709
Nikkaji Number:J2.678.319D
Wikidata:Q82165612
Mol file:73220-53-8.mol

Synonyms:9-(CHLORODIPHENYLSILYL)-9H-FLUORENE;73220-53-8;chloro-(9H-fluoren-9-yl)-diphenylsilane;SCHEMBL6656917;DTXSID70376709;QUYDSKYNFIMLFU-UHFFFAOYSA-N;9-(Diphenylchlorosilyl)-9H-fluorene;Chlorodiphenyl-1-(9-fluorenyl)silane;FT-0762326

Suppliers and Price of 9-(Chlorodiphenylsilyl)-9H-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
9-(CHLORODIPHENYLSILYL)-9H-FLUORENE 95.00%
5MG
$ 505.89

Total 7 raw suppliers

Chemical Property of 9-(Chlorodiphenylsilyl)-9H-fluorene

Chemical Property:

Vapor Pressure:3.61E-10mmHg at 25°C
Refractive Index:1.669
Boiling Point:514.1 °C at 760 mmHg
Flash Point:233 °C
PSA：0.00000
Density:1.22 g/cm³
LogP:5.43230
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:382.0944548
Heavy Atom Count:27
Complexity:453

Purity/Quality:

98%Min ^*data from raw suppliers

9-(CHLORODIPHENYLSILYL)-9H-FLUORENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Si](C2C3=CC=CC=C3C4=CC=CC=C24)(C5=CC=CC=C5)Cl

Technology Process of 9-(Chlorodiphenylsilyl)-9H-fluorene

There total 4 articles about 9-(Chlorodiphenylsilyl)-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 82438-50-4
9-fluorenyllithium

: 80-10-4
diphenylsilyl dichloride

: 73220-53-8
choro(fluoren-9-yl)diphenylsilane

Guidance literature:: In pentane;
DOI:10.1016/S0022-328X(98)00538-5

Reference yield: 59.0%

: diphenylsilylene(9-fluorenyl)(2-methyl-1-indenyl) zirconium dichloride

: 73220-53-8
choro(fluoren-9-yl)diphenylsilane

Guidance literature:

Reference yield:

: 86-73-7
9H-fluorene

: 80-10-4
diphenylsilyl dichloride

: 73220-53-8
choro(fluoren-9-yl)diphenylsilane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, hexane, RT, 2 h, 2.) pentane, RT, 1 h;
DOI:10.1016/0022-328X(95)05788-Q