Technology Process of C17H18N2O4
There total 6 articles about C17H18N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
morpholine;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c2cc35522a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / ethanol / 247 h / 20 °C / Inert atmosphere
2: sodium carbonate / 1,4-dioxane; water / 16 h / 20 °C / Inert atmosphere
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 12 h / Inert atmosphere; Reflux
4: morpholine / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
morpholine; sodium tetrahydroborate; sodium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1039/c2cc35522a
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 12 h / Inert atmosphere; Heating
2: ethanol / 24 h / 20 °C / Inert atmosphere
3: sodium tetrahydroborate / ethanol / 247 h / 20 °C / Inert atmosphere
4: sodium carbonate / 1,4-dioxane; water / 16 h / 20 °C / Inert atmosphere
5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 12 h / Inert atmosphere; Reflux
6: morpholine / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
morpholine; sodium tetrahydroborate; sodium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1039/c2cc35522a
