N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

Base Information

Chemical Name:N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide
CAS No.:1429012-22-5
Molecular Formula:C₂₂H₂₂N₄S
Molecular Weight:374.509
Hs Code.:

Synonyms:N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

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Chemical Property of N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

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Technology Process of N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

There total 1 articles about N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1429012-17-8
N′-(3-cyano-4-iodo-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

: 103-67-3
benzyl-methyl-amine

: 1429012-22-5
N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 100 ℃; for 36h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.02.006

Reference yield: 53.0%

: 1429012-22-5
N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

: 1429012-32-7
N₅-benzyl-N₅-methyl-6-phenylthieno[2,3-d]pyrimidine-4,5-diamine

Guidance literature:: With formamide; at 130 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.02.006

Reference yield:

: 1429012-22-5
N′-(4-(benzyl(methyl)amino)-3-cyano-5-phenylthiophen-2-yl)-N,N-dimethylformimidamide

: C₂₁H₂₂N₄O₆P₂S

Guidance literature:: Multi-step reaction with 3 steps

1: formamide / 48 h / 130 °C / Inert atmosphere

2: toluene / 48 h / 130 °C / Inert atmosphere; Sealed tube; Darkness

3: trimethylsilyl bromide / dichloromethane / 0 - 20 °C

With trimethylsilyl bromide; formamide; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2013.02.006