1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol

Base Information

Chemical Name:1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol
CAS No.:186382-59-2
Molecular Formula:C₂₁H₂₄O₄
Molecular Weight:340.419
Hs Code.:

Synonyms:1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol

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Chemical Property of 1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol

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Technology Process of 1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol

There total 1 articles about 1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: (1S,2S,5S,6R)-5,6-Bis-benzyloxy-2-methoxy-3-tributylstannanyl-cyclohex-3-enol

: 186382-59-2
1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol

Guidance literature:: With sodium methylate; In methanol; at 60 ℃; for 4h;
DOI:10.1016/S0957-4166(96)00461-2

Reference yield:

: 186382-59-2
1D-(1,2,3,4)-1,2-di-O-benzyl-4-O-methylcyclohex-5-ene-1,2,3,4-tetraol

: 10284-63-6
pinitol

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: aq. OsO₄, Me₃NO / acetone; 2-methyl-propan-2-ol / 48 h

3: 58 percent / benzene / 1 h / Ambient temperature

4: 91 percent / K₂CO₃ / methanol / 2 h / 60 °C

5: 69 percent / H₂ / 10percent Pd/C / methanol / 24 h

With pyridine; osmium(VIII) oxide; trimethylamine-N-oxide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; acetone; tert-butyl alcohol; benzene;
DOI:10.1016/S0957-4166(96)00461-2