7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

Base Information

Chemical Name:7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole
CAS No.:1357150-63-0
Molecular Formula:C₅₇H₄₂N₂
Molecular Weight:754.974
Hs Code.:

Synonyms:7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

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Chemical Property of 7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

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Technology Process of 7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

There total 4 articles about 7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.6%

: 952431-30-0
N-[1,1-biphenyl]-4-yl-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-[1,1-biphenyl]-4-amine

: 1257220-44-2
7-bromo-12,12-dimethyl-10-phenyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 1357150-63-0
7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 73 ℃; for 8h; Inert atmosphere;

Reference yield:

: 1357150-72-1
N-(2-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine

: 1357150-63-0
7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: potassium acetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 11 h / 100 °C / Inert atmosphere

2: sodium hydrogensulfite; copper; 3,5-ditertbutyl salicylic acid; potassium carbonate / 10 h / 170 °C / Inert atmosphere

3: N-Bromosuccinimide / N,N-dimethyl-formamide

4: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 8 h / 73 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 3,5-ditertbutyl salicylic acid; potassium acetate; copper; potassium carbonate; sodium hydrogensulfite; In ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1257220-47-5
12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 1357150-63-0
7-[4-{bis(biphenyl-4-yl)amino}-phenyl]-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogensulfite; copper; 3,5-ditertbutyl salicylic acid; potassium carbonate / 10 h / 170 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide

3: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 8 h / 73 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 3,5-ditertbutyl salicylic acid; copper; potassium carbonate; sodium hydrogensulfite; In ethanol; water; N,N-dimethyl-formamide; toluene;